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Polymer-Supported Reagents and 1H-19F NMR Couplings: The Synthesis of 2-Fluoroacetophenone.

  • Autores: Nicola Pohl, Kimberly Schwarz
  • Localización: Journal of chemical education, ISSN 0021-9584, Vol. 85, Nº 6, 2008, págs. 834-835
  • Idioma: inglés
  • Texto completo no disponible (Saber más ...)
  • Resumen
    • We describe an experiment for the undergraduate organic laboratory curriculum in which 2-bromoacetophenone is converted to 2-fluoroacetophenone using a solid-phase nucleophilic fluorine source. The experiment introduces students to the utility of solid-phase reagents in organic synthesis, to NMR-active nuclei other than 1H without the requirement of a special NMR probe, and to the unique uses of fluorine in molecular design.


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